DAVID, Bohumil, Naděžda PIZÚROVÁ, Petr SYNEK, Vít KUDRLE, Ondřej JAŠEK and Oldřich SCHNEEWEISS. epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch. Materials Letters. Amsterdam, Holandsko: Elsevier Science, 2014, vol. 116, February, p. 370-373. ISSN 0167-577X.
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Basic information
Original name epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch
Authors DAVID, Bohumil (203 Czech Republic), Naděžda PIZÚROVÁ (203 Czech Republic), Petr SYNEK (203 Czech Republic, guarantor, belonging to the institution), Vít KUDRLE (203 Czech Republic, belonging to the institution), Ondřej JAŠEK (203 Czech Republic, belonging to the institution) and Oldřich SCHNEEWEISS (203 Czech Republic).
Edition Materials Letters, Amsterdam, Holandsko, Elsevier Science, 2014, 0167-577X.
Other information
Original language English
Type of outcome Article in a journal
Field of Study Plasma physics and discharge through gases
Country of publisher Netherlands
Confidentiality degree is not subject to a state or trade secret
WWW URL URL
RIV identification code RIV/00216224:14740/14:00073662
Organization Středoevropský technologický institut – Repository – Repository
UT WoS 000331025500100
Keywords in English epsilon-Fe2O3; Nanoparticles; Microwave plasma; Mössbauer spectroscopy
Links ED1.1.00/02.0068, research and development project. ED2.1.00/03.0086, research and development project. GAP205/10/1374, research and development project. GA202/08/0178, research and development project.
Changed by Changed by: RNDr. Daniel Jakubík, učo 139797. Changed: 1/9/2020 20:27.
Abstract
The article reports on epsilon-Fe2O3 nanoparticles synthesized in a single step by atmospheric-pressure microwave torch discharge using gaseous precursors only. Morphology and composition of the as-synthesized nanopowder were studied by HR-TEM, XRD, and Mossbauer spectroscopy. In the studied nanopowder, epsilon-Fe2O3 phase (d(xRD)=25 nm, 32 wt%) together with alpha-Fe2O3 and gamma-Fe2O3 phases was found. The characteristic epsilon-Fe2O3 and alpha/gamma-Fe2O3 sextets in the Mossbauer spectra measured at 293 and 5 K confirmed the phase composition of the powder. Compared with the methods currently used for the synthesis of epsilon-Fe2O3 nanoparticles, atmospheric-pressure microwave torch discharge appears as a new synthesis route for obtaining epsilon-Fe2O3 nanoparticles. (C) 2013 Elsevier B.V. All rights reserved.
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