J 2024

Merging Bambus[6]uril and Biotin[6]uril into an Enantiomerically Pure Monofunctionalized Hybrid Macrocycle

DEL MAURO, Arico; Jana LAPEŠOVÁ; Carola RANDO and Vladimír ŠINDELÁŘ

Basic information

Original name

Merging Bambus[6]uril and Biotin[6]uril into an Enantiomerically Pure Monofunctionalized Hybrid Macrocycle

Authors

DEL MAURO, Arico; Jana LAPEŠOVÁ; Carola RANDO and Vladimír ŠINDELÁŘ

Edition

Organic Letters, WASHINGTON, American Chemical Society, 2024, 1523-7060

Other information

Language

English

Type of outcome

Article in a journal

Country of publisher

United States of America

Confidentiality degree

is not subject to a state or trade secret

References:

URL

Marked to be transferred to RIV

Yes

RIV identification code

RIV/00216224:14310/24:00135408

Organization

Přírodovědecká fakulta – Repository – Repository

DOI

https://doi.org/10.1021/acs.orglett.3c03715

UT WoS

001143342500001

EID Scopus

2-s2.0-85181580836

Keywords in English

Anions; Carboxyls; Cavities; Macrocycles; Supramolecular chemistry

Links

EF17_043/0009632, research and development project. GA23-05271S, research and development project. MUNI/A/1604/2023, interní kód Repo. 857560, interní kód Repo. RECETOX RI, large research infrastructures. CIISB II, large research infrastructures. CZ-OPENSCREEN IV, large research infrastructures.
Changed: 8/5/2025 00:50, RNDr. Daniel Jakubík

Abstract

In the original language

Bambus-[6]-urils and biotin[6]-urils are macrocycles with an exceptional affinity for inorganic anions. Here, we investigated statistical condensation of 2,4-dibenzylglycoluril and d-biotin, monomers of the corresponding macrocycles, to prepare the enantiomerically pure macrocycle 1 containing a single d-biotin and five glycoluril units. Host-guest properties of 1 in chloroform solution and solid state were investigated. The macrocycle 1 bearing a single functional group was employed in the formation of [1]-rotaxane utilizing reversible covalent bonds.
Displayed: 3/5/2026 04:30